Rapid urbanization and increased anthropogenic activities have intensified air pollution in
many Nigerian cities, posing significant environmental and public health risks. This study
comparatively evaluated ambient air pollution levels in Owerri urban and its surrounding
environments in southeastern Nigeria. Seven sampling locations representing urban, peri
urban, and relatively less disturbed areas were selected for field monitoring. Concentrations
of major atmospheric pollutants including hydrogen sulphide (H₂S), nitrogen dioxide (NO₂),
carbon dioxide (CO₂), carbon monoxide (CO), volatile organic compounds (VOCs),
particulate matter (PM₂.₅) and particulate matter (PM₁₀) were measured using portable air
quality monitoring instruments. Spatial coordinates were recorded using a Global Positioning
System and spatial distribution patterns were analyzed using Inverse Distance Weighted
interpolation within a Geographic Information System environment. Results revealed
considerable spatial variation in pollutant concentrations across the study area. Carbon
dioxide exhibited the highest overall concentrations, indicating the dominance of combustion
related activities. Elevated concentrations of CO, PM₂.₅ and PM₁₀ were observed around high
traffic and commercial locations, particularly around the World Bank, Orji and Egbu axes of
Owerri. Lower concentrations were recorded in less densely populated peripheral areas. The
spatial analysis revealed distinct pollution hotspots associated with vehicular emissions,
generator use, road dust resuspension and commercial activities. The study highlights the
growing air quality challenges in Owerri and recommends continuous air quality monitoring,
stricter emission control policies and sustainable urban planning strategies to mitigate
pollution and protect public health.